Difference between revisions of "Walk-up NMR user instructions for ThermoFisher"

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The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
 
The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
 +
# Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
 +
# Check to make sure a filter is properly connected and a collection flask is at the "out" port.
 +
# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.
  
 
[[File:picospin.jpg|400px]]
 
[[File:picospin.jpg|400px]]

Revision as of 09:07, 20 May 2020

The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:

  1. Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
  2. Check to make sure a filter is properly connected and a collection flask is at the "out" port.
  3. Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.

Picospin.jpg