Difference between revisions of "Walk-up NMR user instructions for ThermoFisher"
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The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample: | The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample: | ||
| + | # Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present. | ||
| + | # Check to make sure a filter is properly connected and a collection flask is at the "out" port. | ||
| + | # Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port. | ||
[[File:picospin.jpg|400px]] | [[File:picospin.jpg|400px]] | ||
Revision as of 09:07, 20 May 2020
The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
- Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
- Check to make sure a filter is properly connected and a collection flask is at the "out" port.
- Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.
