Walk-up NMR user instructions for ThermoFisher - Revision history

Milllo at 09:37, 25 May 2020

2020-05-25T09:37:32Z

← Older revision		Revision as of 03:37, 25 May 2020
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	The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:		The [[NMR Instrument Manufacturers\|picospin]] tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
	# Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.		# Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
	# Check to make sure a filter is properly connected and a collection flask is at the "out" port.		# Check to make sure a filter is properly connected and a collection flask is at the "out" port.

2020-05-22T06:47:01Z

← Older revision		Revision as of 00:47, 22 May 2020
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	# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.		# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.
	# Go to the picospin page of the web browser interface		# Go to the picospin page of the web browser interface
	# Select the '''Files'''option.		# Select the '''Files''' option.
	# Select the '''Standard Run''' option.		# Select the '''Standard Run''' option.
	# Click '''Use these settings at run'''.		# Click '''Use these settings at run'''.

2020-05-20T15:12:18Z

← Older revision		Revision as of 09:12, 20 May 2020
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	# Check to make sure a filter is properly connected and a collection flask is at the "out" port.		# Check to make sure a filter is properly connected and a collection flask is at the "out" port.
	# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.		# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.
			# Go to the picospin page of the web browser interface
			# Select the '''Files'''option.
			# Select the '''Standard Run''' option.
			# Click '''Use these settings at run'''.
			# The '''Run''' page will appear.
			# Check the transmitter frequency and set the scans.
			# Click '''Start Run'''.
			# Process spectra with MNova, which is included with the product.



	[[File:picospin.jpg\|400px]]		[[File:picospin.jpg\|400px]]

2020-05-20T15:07:28Z

← Older revision		Revision as of 09:07, 20 May 2020
Line 3:		Line 3:
	# Check to make sure a filter is properly connected and a collection flask is at the "out" port.		# Check to make sure a filter is properly connected and a collection flask is at the "out" port.
	# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.		# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.



	[[File:picospin.jpg\|400px]]		[[File:picospin.jpg\|400px]]

2020-05-20T15:07:10Z

← Older revision		Revision as of 09:07, 20 May 2020
Line 1:		Line 1:
	The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:		The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
			# Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
			# Check to make sure a filter is properly connected and a collection flask is at the "out" port.
			# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.

	[[File:picospin.jpg\|400px]]		[[File:picospin.jpg\|400px]]

2020-05-20T15:01:09Z

← Older revision		Revision as of 09:01, 20 May 2020
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	The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing.		The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:

	[[File:picospin.jpg\|400px]]		[[File:picospin.jpg\|400px]]

2020-05-20T14:59:48Z

← Older revision		Revision as of 08:59, 20 May 2020
Line 1:		Line 1:
	The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing.		The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing.

			[[File:picospin.jpg\|400px]]

2020-05-20T14:48:56Z

← Older revision		Revision as of 08:48, 20 May 2020
Line 1:		Line 1:
	The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes.		The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing.

2020-05-20T14:39:52Z

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The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes.