Walk-up NMR user instructions for Bruker - Revision history

Milllo: /* Introduction */

2020-05-25T09:33:08Z

Introduction

Milllo: /* Introduction */

2020-05-25T09:31:08Z

Introduction

Milllo: /* Step by step */

2020-05-20T15:46:29Z

Step by step

Milllo: /* Step by step */

2020-05-19T10:19:51Z

Step by step

Milllo: /* Step by step */

2020-05-19T10:19:01Z

Step by step

Milllo: /* Step by step */

2020-05-19T10:18:00Z

Step by step

Milllo: /* Step by step */

2020-05-19T10:09:09Z

Step by step

Milllo at 05:45, 19 May 2020

2020-05-19T05:45:31Z

Milllo: /* Introduction */

2020-05-19T01:05:07Z

Introduction

Milllo: /* Step by step */

2020-05-14T14:36:23Z

Step by step

@@ Line 1: / Line 1: @@
 ==Introduction==
-If you need to use a [http://www.apimba.org/mediawiki/index.php?title=NMR_Instrument_Manufacturers Bruker] NMR instrument for a liquid sample, here are some instructions to get a quick spectrum of your sample. Samples for most Bruker high frequency magnets use regular 5mm NMR tubes.
+If you need to use a [[NMR Instrument Manufacturers|Bruker]] NMR instrument for a liquid sample, here are some instructions to get a quick spectrum of your sample. Samples for most Bruker high frequency magnets use regular 5mm NMR tubes.
 ==Step by step==

@@ Line 1: / Line 1: @@
 ==Introduction==
-If you need to use a Bruker NMR instrument for a liquid sample, here are some instructions to get a quick spectrum of your sample. Samples for most Bruker high frequency magnets use regular 5mm NMR tubes.
+If you need to use a [http://www.apimba.org/mediawiki/index.php?title=NMR_Instrument_Manufacturers Bruker] NMR instrument for a liquid sample, here are some instructions to get a quick spectrum of your sample. Samples for most Bruker high frequency magnets use regular 5mm NMR tubes.
 ==Step by step==

@@ Line 11: / Line 11: @@
 # place the sample/spinner in the depth gauge.
 # slide your sample down in the spinner until it hits the stop of the gauge.
-# place the sample/holder on top of the column of air on the magnet.
+# place the sample/spinner on top of the column of air on the magnet.
 # go back to the workstation, type '''ij''' on the command line or click the '''insert''' button and wait for the sample to drop down into the probe.
 # type '''lock''' on the command line.

@@ Line 5: / Line 5: @@
 # log in to workstation.
 # log in to TopSpin.
-# type '''ej''' on the command line or click the eject button to eject the current sample that is in the magnet.
+# type '''ej''' on the command line or click the '''eject''' button to eject the current sample that is in the magnet.
 # remove the old sample from the top of the magnet.
 # remove the old sample from the spinner.
@@ Line 12: / Line 12: @@
 # slide your sample down in the spinner until it hits the stop of the gauge.
 # place the sample/holder on top of the column of air on the magnet.
-# go back to the workstation, type '''ij''' on the command line or click insert sample and wait for the sample to drop down into the probe.
+# go back to the workstation, type '''ij''' on the command line or click the '''insert''' button and wait for the sample to drop down into the probe.
 # type '''lock''' on the command line.
 # when the list of solvents appears, choose the one that your sample is in. Wait for locking.

@@ Line 12: / Line 12: @@
 # slide your sample down in the spinner until it hits the stop of the gauge.
 # place the sample/holder on top of the column of air on the magnet.
-# go back to the workstation, click insert sample and wait for the sample to drop down into the probe.
+# go back to the workstation, type '''ij''' on the command line or click insert sample and wait for the sample to drop down into the probe.
 # type '''lock''' on the command line.
 # when the list of solvents appears, choose the one that your sample is in. Wait for locking.

@@ Line 7: / Line 7: @@
 # type '''ej''' on the command line or click the eject button to eject the current sample that is in the magnet.
 # remove the old sample from the top of the magnet.
-# remove the old sample from the sample holder.
+# remove the old sample from the spinner.
-# place your sample in the sample holder.
+# place your sample in the spinner.
 # slide your sample down in the holder until it hits the stop.
 # place the sample/holder on top of the column of air on the magnet.

@@ Line 14: / Line 14: @@
 # type '''lock''' on the command line.
 # when the list of solvents appears, choose the one that your sample is in. Wait for locking.
-# once the sample is locked, type topshim on the command line to shim the sample.
+# once the sample is locked, type '''topshim''' on the command line to shim the sample.
-# while the sample is being automatically shimmed, type edc on the command line to create a new dataset.
+# while the sample is being automatically shimmed, type '''edc''' on the command line to create a new dataset.
-# edc opens the window that sets everything for the experiment to run your sample (example [[New Dataset Window for Bruker TopSpin|here]]).
+# '''edc''' opens the window that sets everything for the experiment to run your sample (example [[New Dataset Window for Bruker TopSpin|here]]).
-# The NAME field is usually a sample# from a logbook, while a description of the sample goes into the TITLE field.
+# The '''NAME''' field is usually a sample# from a logbook, while a description of the sample goes into the '''TITLE''' field.
-# The Experiment field is where the pulse program is chosen. Each facility has their own program that is customized for their instrument.
+# The '''Experiment''' field is where the pulse program is chosen. Each facility has their own program that is customized for their instrument.
 # The other fields are usually left at default since they are set by the instrument administrator.
-# Set the number of scans by typing ns in the command line.
+# Set the number of scans by typing '''ns''' in the command line.
-# Type zg on the command line to start the run.
+# Type '''zg''' on the command line to start the run.
-# When the run is finished, type efp, apk, absn to process into a spectrum.
+# When the run is finished, type '''efp''', '''apk''' and '''absn''' to process into a spectrum.